NMR Services
Nuclear Magnetic Resonance Spectroscopy Unit
We offer solutions to your problems in determining short range atomic topology in condensed matter. We have long-standing experience in investigating fuel cell components, superconductors, zeolites, oil shale products, proteins, various bio- and synthetic polymers and different biologically active compounds, to name a few.
Contact persons:
Indrek Reile, PhD (indrek.reile@kbfi.ee)
Jasper Adamson, PhD (jasper.adamson@kbfi.ee) – high-resolution solution NMR
Ivo Heinmaa, PhD (ivo.heinmaa@kbfi.ee) – solid state NMR
Jüri Jarvet, PhD (Jyri.jarvet@kbfi.ee) – bioNMR
Tõnis Pehk, DrSci (tonis.pehk@kbfi.ee) – high-resolution solution NMR
Facilities
The Laboratory has four research grade Bruker NMR spectrometers that cover a range of frequencies, nuclei and a diversity of applications.
AVANCE III 800MHz (18.8T magnetic field) installed September 2007
Features: Advanced multidimensional experiments
Triple resonance 1H/13C/15N PFG probehead
Dual 1H/13C PFG probehead
Solid state triple resonance 1H/13C/15N probehead
BBO probe 1H/19F, broadband range 31P 109Ag
QCI CryoProbe
SampleXpress Sample Changer
AVANCE II 600MHz (14.1 T magnetic field); installed 2000, last upgrade 2005
Features Advanced multidimensional experiments
Triple resonance 1H/13C/15N PFG probehead
Solid state probes 1-6 mm and DOR probehead
AMX 500 (11.7T magnetic field); installed 1985, last upgrade 2010
Features: Liquid 1H/13C probehead
CXP 360 spectrometer attached to 8.5T or 4.7T WB-magnets
Features: Solid state / low / high temperature (10 <t
The Lab has access to cryogenic liquids and compressed He gas for low temperature work.